What Are the Standard Size and Shape Specifications for Sample Containers in DTA?
Sample containers must fit exactly in the instrument and work with automated or manual handling systems. Standard sizing means no lost samples or off-center runs.
DTA sample containers usually follow industry norms for diameter, height, and wall thickness. Uniform shape enables repeatable heating and stable sample location, which is critical for trusted measurements (Differential Thermal Analysis).
| Specification | Typical Range | Importance | Application |
|---|---|---|---|
| Outer diameter | 5–8 mm | Instrument fit, heat contact | Standard DTA holders |
| Height/depth | 2–6 mm | Holds full sample | Surface vs. bulk samples |
| Wall thickness | 0.1–0.3 mm | Thermal conduction | Fast response time |
| Shape type | Cylindrical, pan, crucible | Uniform heating | Various DTA models |
How Does the Material Composition Affect the Performance of Sample Containers in DTA?
The wrong material can cause melting, contamination, or bad sensitivity. The right choice protects your lab and guarantees measurement reliability across temperatures.
Platinum, aluminum, and ceramic are leading materials for DTA containers. Platinum gives unmatched purity and heat resistance. Aluminum supports affordable routine work. Ceramics handle harsh chemistries well. Selection should match your sample and test environment (Platinum).
| Material | Thermal Conductivity | Max Working Temp (°C) | Reactivity | Best Use |
|---|---|---|---|---|
| Platinum | High | 1600 | Inert | High-temp, sensitive |
| Aluminum | Very high | 630 | Low to moderate | Routine DTA, organics |
| Ceramic | Moderate | 1700 | Low | Aggressive samples |
What Temperature Range Can Sample Containers for DTA Withstand?
Not every container works at every temperature. Using a pan above its limit can risk tests, samples, and your whole instrument.
DTA sample containers are designed and tested to survive their maximum rated temperatures. Platinum containers lead at high heat. Quality aluminum pans work for standard organic tests. Ceramics are chosen for high or unusual temperature conditions (thermal analysis).
| Material Type | Max Use Temp (°C) | Failure Mode | Key Use Case |
|---|---|---|---|
| Platinum | 1600 | No melt/deform | Pharma, electronics |
| Aluminum | 630 | Melting, loss of shape | Routine, food, organic |
| Ceramic | 1700 | May crack, but does not melt | Batteries, chemicals |
What Precision Tolerances Are Required for Sample Containers in Thermal Analysis?
Precision tolerance means keeping dimensions as close as possible to spec. Tight tolerance matters more when test repeatability and automation are part of the workflow.
Low tolerance on size, thickness, and mass ensures all DTA pans sit flat, seal right, and deliver even heat. Good control lets researchers compare old and new data without error (engineering tolerance).
| Tolerance Spec | Recommended Value | Why It Matters | Consequence if Missed |
|---|---|---|---|
| Diameter | ±0.01 mm | Instrument fit, heat flow | Loose fit, skewed data |
| Height | ±0.02 mm | Volume, consistent mass | Wrong sample depth |
| Thickness | ±0.005 mm | Steady response | Baseline drift |
| Weight | ±0.1% | Stable mass balance | Long-term drift |







